2,3-Dichlorobenzene-1-sulfonyl chloride → HCID 10287052, compound

HRID 1443937Notes

Reaction equation

HRID 1443937 reaction equation
[Cl:1][C:2]1[N:7]=[C:6]([NH2:8])[C:5]([O:9][CH3:10])=[N:4][CH:3]=1.[Cl:11][C:12]1[C:17]([Cl:18])=[CH:16][CH:15]=[CH:14][C:13]=1[S:19](Cl)(=[O:21])=[O:20]>>[Cl:11][C:12]1[C:17]([Cl:18])=[CH:16][CH:15]=[CH:14][C:13]=1[S:19]([NH:8][C:6]1[C:5]([O:9][CH3:10])=[N:4][CH:3]=[C:2]([Cl:1])[N:7]=1)(=[O:21])=[O:20]

Participants

3

Reactant 2

HCID 27342222,3-Dichlorobenzene-1-sulfonyl chlorideHCID 179559946-Chloro-3-methoxypyrazin-2-amine

Product 1

HCID 10287052HCID 10287052, compound

Procedure

Prepared by the method of Example 1 (reaction performed at room temperature) using 6-chloro-3-methoxy-2-pyrazinamine (0.24 g) and 2,3-dichlorobenzenesulphonyl chloride (0.32 g). Yield 0.24 g.

Workup

  1. customPrepared by the method of Example 1 (reaction performed at room temperature)

Sources & evidence

ORD record
ord-cbde71eb71e64ed083d16b9a533e67f5
Source dataset
uspto-grants-2010_02
Patent number
US07662825B2

Reaction notes

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