3,5-Dichlorobenzenesulfonyl chloride → HCID 10309892, compound

HRID 1443940Notes

Reaction equation

HRID 1443940 reaction equation
[Br:1][C:2]1[N:3]=[C:4]([O:9][CH3:10])[C:5]([NH2:8])=[N:6][CH:7]=1.[Cl:11][C:12]1[CH:13]=[C:14]([S:19](Cl)(=[O:21])=[O:20])[CH:15]=[C:16]([Cl:18])[CH:17]=1>>[Br:1][C:2]1[N:3]=[C:4]([O:9][CH3:10])[C:5]([NH:8][S:19]([C:14]2[CH:13]=[C:12]([Cl:11])[CH:17]=[C:16]([Cl:18])[CH:15]=2)(=[O:21])=[O:20])=[N:6][CH:7]=1

Participants

3

Reactant 2

HCID 5223883,5-Dichlorobenzenesulfonyl chlorideHCID 113447242-Amino-5-bromo-3-methoxypyrazine

Product 1

HCID 10309892HCID 10309892, compound

Procedure

Prepared by the method of Example 1 (reaction performed at room temperature) using 5-bromo-3-methoxy-2-pyrazinamine (0.2 g) and 3,5-dichlorobenzenesulphonyl chloride (0.24 g). Yield 0.012 g.

Workup

  1. customPrepared by the method of Example 1 (reaction performed at room temperature)

Sources & evidence

ORD record
ord-4383c73cd7a5487683cb910fefc6880b
Source dataset
uspto-grants-2010_02
Patent number
US07662825B2

Reaction notes

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