Benzenesulfonyl chloride, 3,4-dichloro- → HCID 10194488, compound

HRID 1443943Notes

Reaction equation

HRID 1443943 reaction equation
[Br:1][C:2]1[N:3]=[C:4]([O:9][CH3:10])[C:5]([NH2:8])=[N:6][CH:7]=1.[Cl:11][C:12]1[CH:13]=[C:14]([S:19](Cl)(=[O:21])=[O:20])[CH:15]=[CH:16][C:17]=1[Cl:18]>>[Br:1][C:2]1[N:3]=[C:4]([O:9][CH3:10])[C:5]([NH:8][S:19]([C:14]2[CH:15]=[CH:16][C:17]([Cl:18])=[C:12]([Cl:11])[CH:13]=2)(=[O:21])=[O:20])=[N:6][CH:7]=1

Participants

3

Reactant 2

HCID 7383Benzenesulfonyl chloride, 3,4-dichloro-HCID 113447242-Amino-5-bromo-3-methoxypyrazine

Product 1

HCID 10194488HCID 10194488, compound

Procedure

Prepared by the method of Example 1 (reaction performed at room temperature) using 5-bromo-3-methoxy-2-pyrazinamine (0.15 g) and 3,4-dichlorobenzenesulphonyl chloride (0.15 g). Yield 0.09 g.

Workup

  1. customPrepared by the method of Example 1 (reaction performed at room temperature)

Sources & evidence

ORD record
ord-94fc38548be34d5d9e2ec329a1ab7136
Source dataset
uspto-grants-2010_02
Patent number
US07662825B2

Reaction notes

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