3-Chlorobenzenesulphonyl chloride → HCID 59168189, compound

HRID 1443945Notes

Reaction equation

HRID 1443945 reaction equation
[Br:1][C:2]1[N:3]=[C:4]([O:9][CH3:10])[C:5]([NH2:8])=[N:6][CH:7]=1.[Cl:11][C:12]1[CH:13]=[C:14]([S:18](Cl)(=[O:20])=[O:19])[CH:15]=[CH:16][CH:17]=1>>[Br:1][C:2]1[N:3]=[C:4]([O:9][CH3:10])[C:5]([NH:8][S:18]([C:14]2[CH:15]=[CH:16][CH:17]=[C:12]([Cl:11])[CH:13]=2)(=[O:20])=[O:19])=[N:6][CH:7]=1

Participants

3

Reactant 2

HCID 179093-Chlorobenzenesulphonyl chlorideHCID 113447242-Amino-5-bromo-3-methoxypyrazine

Product 1

HCID 59168189HCID 59168189, compound

Procedure

Prepared by the method of Example 1 (reaction performed at room temperature) using 5-bromo-3-methoxy-2-pyrazinamine (0.1 g) and 3-chlorobenzenesulphonyl chloride (0.13 g).

Workup

  1. customPrepared by the method of Example 1 (reaction performed at room temperature)

Sources & evidence

ORD record
ord-4557837d772940d28afb6f7e3e65a5f1
Source dataset
uspto-grants-2010_02
Patent number
US07662825B2

Reaction notes

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