2-Iodobenzene-1-sulfonyl chloride → N-(5-Bromo-3-methoxy-2-pyrazinyl)2-iodobenzenesulphonamide

HRID 1443952Notes

Reaction equation

HRID 1443952 reaction equation
[Br:1][C:2]1[N:3]=[C:4]([O:9][CH3:10])[C:5]([NH2:8])=[N:6][CH:7]=1.[I:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=1[S:18](Cl)(=[O:20])=[O:19]>>[Br:1][C:2]1[N:3]=[C:4]([O:9][CH3:10])[C:5]([NH:8][S:18]([C:13]2[CH:14]=[CH:15][CH:16]=[CH:17][C:12]=2[I:11])(=[O:20])=[O:19])=[N:6][CH:7]=1

Participants

3

Reactant 2

HCID 6274002-Iodobenzene-1-sulfonyl chlorideHCID 113447242-Amino-5-bromo-3-methoxypyrazine

Product 1

HCID 59168097N-(5-Bromo-3-methoxy-2-pyrazinyl)2-iodobenzenesulphonamide

Procedure

Prepared by the method of Example 1 (reaction performed at room temperature) using 5-bromo-3-methoxy-2-pyrazinamine and 2-iodobenzenesulphonyl chloride.

Workup

  1. customPrepared by the method of Example 1 (reaction performed at room temperature)

Sources & evidence

ORD record
ord-0f59945477aa47dda7d725247d383249
Source dataset
uspto-grants-2010_02
Patent number
US07662825B2

Reaction notes

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