3-Pyridinemethanol → HCID 59168127, compound

HRID 1443963Notes

Reaction equation

[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([CH2:7][OH:8])[CH:2]=1.[Cl:9][C:10]1[C:15]([Cl:16])=[CH:14][CH:13]=[CH:12][C:11]=1[S:17]([NH:20][C:21]1[C:26](Cl)=[N:25][CH:24]=[CH:23][N:22]=1)(=[O:19])=[O:18]>>[Cl:9][C:10]1[C:15]([Cl:16])=[CH:14][CH:13]=[CH:12][C:11]=1[S:17]([NH:20][C:21]1[C:26]([O:8][CH2:7][C:3]2[CH:2]=[N:1][CH:6]=[CH:5][CH:4]=2)=[N:25][CH:24]=[CH:23][N:22]=1)(=[O:18])=[O:19]

Participants

Reactant 2

HCID 75103-Pyridinemethanol

HCID 591681672,3-Dichloro-N-(3-chloro-2-pyrazinyl)benzenesulphonamide

Product 1

HCID 59168127HCID 59168127, compound

Procedure

Prepared by the method of Example 28 using pyridine-3-methanol (0.09 g) and 2,3-dichloro-N-(3-chloro-2-pyrazinyl)benzenesulphonamide (0.1 g). Yield 0.042 g.

Sources & evidence

ORD record: ord-3984cf65ae19403cbddd5b4066ae7a11
Source dataset: uspto-grants-2010_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07662825B2

Reaction notes

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