3-Chloro-2-methylbenzenesulfonyl chloride → HCID 59168158, compound

HRID 1443971Notes

Reaction equation

HRID 1443971 reaction equation
[Cl:1][C:2]1[N:3]=[C:4]([O:9][CH3:10])[C:5]([NH2:8])=[N:6][CH:7]=1.[Cl:11][C:12]1[C:13]([CH3:22])=[C:14]([S:18](Cl)(=[O:20])=[O:19])[CH:15]=[CH:16][CH:17]=1>>[Cl:11][C:12]1[C:13]([CH3:22])=[C:14]([S:18]([NH:8][C:5]2[C:4]([O:9][CH3:10])=[N:3][C:2]([Cl:1])=[CH:7][N:6]=2)(=[O:20])=[O:19])[CH:15]=[CH:16][CH:17]=1

Participants

3

Reactant 2

HCID 5227343-Chloro-2-methylbenzenesulfonyl chlorideHCID 107970362-Amino-5-chloro-3-methoxypyrazine

Product 1

HCID 59168158HCID 59168158, compound

Procedure

Prepared by the method of Example 1 (reaction performed at room temperature) using 5-chloro-3-methoxy-2-pyrazinamine (0.1 g) and 3-chloro-2-methylbenzenesulphonyl chloride (0.15 g). Yield 0.085 g.

Workup

  1. customPrepared by the method of Example 1 (reaction performed at room temperature)

Sources & evidence

ORD record
ord-a1e6e5e929d24778a7ad76668307eb4e
Source dataset
uspto-grants-2010_02
Patent number
US07662825B2

Reaction notes

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