4-Chlorobenzenesulfonyl chloride → HCID 10286642, compound

HRID 1443974Notes

Reaction equation

HRID 1443974 reaction equation
[Cl:1][C:2]1[N:3]=[C:4]([O:9][CH3:10])[C:5]([NH2:8])=[N:6][CH:7]=1.[Cl:11][C:12]1[CH:17]=[CH:16][C:15]([S:18](Cl)(=[O:20])=[O:19])=[CH:14][CH:13]=1>>[Cl:11][C:12]1[CH:17]=[CH:16][C:15]([S:18]([NH:8][C:5]2[C:4]([O:9][CH3:10])=[N:3][C:2]([Cl:1])=[CH:7][N:6]=2)(=[O:20])=[O:19])=[CH:14][CH:13]=1

Participants

3

Reactant 2

HCID 73984-Chlorobenzenesulfonyl chlorideHCID 107970362-Amino-5-chloro-3-methoxypyrazine

Product 1

HCID 10286642HCID 10286642, compound

Procedure

Prepared by the method of Example 1 (reaction performed at room temperature) using 5-chloro-3-methoxy-2-pyrazinamine (0.1 g) and 4-chlorobenzenesulphonyl chloride (0.13 g).

Workup

  1. customPrepared by the method of Example 1 (reaction performed at room temperature)

Sources & evidence

ORD record
ord-c9f01c8664b04e8ebb9859014b69c407
Source dataset
uspto-grants-2010_02
Patent number
US07662825B2

Reaction notes

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