Benzenesulfonyl chloride, 3,4-dichloro- → HCID 59168179, compound
Reaction equation
[Cl:1][C:2]1[N:3]=[C:4]([O:10][CH3:11])[C:5]([NH2:9])=[N:6][C:7]=1[Cl:8].[Cl:12][C:13]1[CH:14]=[C:15]([S:20](Cl)(=[O:22])=[O:21])[CH:16]=[CH:17][C:18]=1[Cl:19]>>[Cl:12][C:13]1[CH:14]=[C:15]([S:20]([NH:9][C:5]2[C:4]([O:10][CH3:11])=[N:3][C:2]([Cl:1])=[C:7]([Cl:8])[N:6]=2)(=[O:21])=[O:22])[CH:16]=[CH:17][C:18]=1[Cl:19]Participants
3
Procedure
Prepared by the method of Example 1 (reaction performed at room temperature) using 5,6-dichloro-3-methoxy-2-pyrazinamine (0.1 g) and 3,4-dichlorobenzenesulphonyl chloride (0.15 g). Yield 0.11 g.
Workup
- customPrepared by the method of Example 1 (reaction performed at room temperature)
Sources & evidence
- ORD record
- ord-641927bf928741d2a7af433b83523e9b
- Source dataset
- uspto-grants-2010_02
- Patent number
- US07662825B2
Reaction notes
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