2,3-Dichlorobenzene-1-sulfonyl chloride → HCID 10193757, compound

HRID 1443985Notes

Reaction equation

HRID 1443985 reaction equation
[CH3:1][O:2][C:3]1[C:4]([NH2:11])=[N:5][C:6]([CH3:10])=[C:7]([CH3:9])[N:8]=1.[Cl:12][C:13]1[C:18]([Cl:19])=[CH:17][CH:16]=[CH:15][C:14]=1[S:20](Cl)(=[O:22])=[O:21]>>[Cl:12][C:13]1[C:18]([Cl:19])=[CH:17][CH:16]=[CH:15][C:14]=1[S:20]([NH:11][C:4]1[C:3]([O:2][CH3:1])=[N:8][C:7]([CH3:9])=[C:6]([CH3:10])[N:5]=1)(=[O:22])=[O:21]

Participants

3

Reactant 2

HCID 27342222,3-Dichlorobenzene-1-sulfonyl chlorideHCID 11321063HCID 11321063, compound

Product 1

HCID 10193757HCID 10193757, compound

Procedure

Prepared by the method of Example 1 using 3-methoxy-5,6-dimethyl-2-pyrazinamine (0.07 g) and 2,3-dichlorobenzenesulphonyl chloride (0.12 g). Yield 0.04 g.

Sources & evidence

ORD record
ord-d3f017ac8e2d445b821b2a33f8e453d5
Source dataset
uspto-grants-2010_02
Patent number
US07662825B2

Reaction notes

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