2-(Methylthio)ethanol → HCID 59168193, compound
Reaction equation
[CH3:1][S:2][CH2:3][CH2:4][OH:5].[Cl:6][C:7]1[C:12]([Cl:13])=[CH:11][CH:10]=[CH:9][C:8]=1[S:14]([NH:17][C:18]1[C:23](Cl)=[N:22][C:21]([Cl:25])=[CH:20][N:19]=1)(=[O:16])=[O:15]>>[Cl:6][C:7]1[C:12]([Cl:13])=[CH:11][CH:10]=[CH:9][C:8]=1[S:14]([NH:17][C:18]1[C:23]([O:5][CH2:4][CH2:3][S:2][CH3:1])=[N:22][C:21]([Cl:25])=[CH:20][N:19]=1)(=[O:16])=[O:15]Participants
3
Procedure
Prepared by the method of Example 31 using 2-methylsulphanylethanol (0.05 g) and 2,3-dichloro-N-(3,5-dichloro-2-pyrazinyl)benzenesulphonamide (Example 74) (0.1 g). Yield 0.06 g.
Sources & evidence
- ORD record
- ord-14fe620f3e394b51bfd3243cf48ba789
- Source dataset
- uspto-grants-2010_02
- Patent number
- US07662825B2
Reaction notes
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