2,3-Dichlorobenzene-1-sulfonyl chloride → HCID 59168150, compound

HRID 1444025Notes

Reaction equation

HRID 1444025 reaction equation
[Cl:1][C:2]1[N:3]=[C:4]([O:10][CH2:11][C:12]2[CH:13]=[N:14][CH:15]=[CH:16][CH:17]=2)[C:5]([NH2:9])=[N:6][C:7]=1[Cl:8].[Cl:18][C:19]1[C:24]([Cl:25])=[CH:23][CH:22]=[CH:21][C:20]=1[S:26](Cl)(=[O:28])=[O:27]>>[Cl:18][C:19]1[C:24]([Cl:25])=[CH:23][CH:22]=[CH:21][C:20]=1[S:26]([NH:9][C:5]1[C:4]([O:10][CH2:11][C:12]2[CH:13]=[N:14][CH:15]=[CH:16][CH:17]=2)=[N:3][C:2]([Cl:1])=[C:7]([Cl:8])[N:6]=1)(=[O:28])=[O:27]

Participants

3

Reactant 2

HCID 27342222,3-Dichlorobenzene-1-sulfonyl chlorideHCID 591682112-Pyrazinamine, 5,6-dichloro-3-(3-pyridinylmethoxy)-

Product 1

HCID 59168150HCID 59168150, compound

Procedure

Prepared by the method of Example 1 (reaction performed at room temperature) using 5,6-dichloro-3-(3-pyridinylmethoxy)-2-pyrazinamine (Example 121a) (0.27 g) and 2,3-dichlorobenzenesulphonyl chloride (0.27 g). Yield 0.17 g.

Workup

  1. customPrepared by the method of Example 1 (reaction performed at room temperature)

Sources & evidence

ORD record
ord-3705aae4c01541f9a5a27bcdc43a1d29
Source dataset
uspto-grants-2010_02
Patent number
US07662825B2

Reaction notes

Loading…