(6-Methoxypyridin-3-yl)methanol → HCID 59168154, compound

HRID 1444030Notes

Reaction equation

HRID 1444030 reaction equation
[Cl:1][C:2]1[C:7]([Cl:8])=[CH:6][CH:5]=[CH:4][C:3]=1[S:9]([NH:12][C:13]1[C:18](Cl)=[N:17][CH:16]=[CH:15][N:14]=1)(=[O:11])=[O:10].[CH3:20][O:21][C:22]1[N:27]=[CH:26][C:25]([CH2:28][OH:29])=[CH:24][CH:23]=1>>[Cl:1][C:2]1[C:7]([Cl:8])=[CH:6][CH:5]=[CH:4][C:3]=1[S:9]([NH:12][C:13]1[C:18]([O:29][CH2:28][C:25]2[CH:26]=[N:27][C:22]([O:21][CH3:20])=[CH:23][CH:24]=2)=[N:17][CH:16]=[CH:15][N:14]=1)(=[O:11])=[O:10]

Participants

3

Reactant 2

HCID 12259941(6-Methoxypyridin-3-yl)methanolHCID 591681672,3-Dichloro-N-(3-chloro-2-pyrazinyl)benzenesulphonamide

Product 1

HCID 59168154HCID 59168154, compound

Procedure

Prepared by the method of Example 28b using 2,3-dichloro-N-(3-chloro-2-pyrazinyl)benzenesulphonamide (Example 28a) (0.338 g) and (6-methoxy-3-pyridinyl)methanol (0.21 g). Yield 0.23 g.

Workup

  1. customPrepared by the method of Example 28b

Sources & evidence

ORD record
ord-1339df2654a84aea87a5b6add40cccb6
Source dataset
uspto-grants-2010_02
Patent number
US07662825B2

Reaction notes

Loading…