Allyl Alcohol → HCID 59168169, compound
Reaction equation
[Cl:1][C:2]1[C:7]([Cl:8])=[CH:6][CH:5]=[CH:4][C:3]=1[S:9]([NH:12][C:13]1[C:18](Cl)=[N:17][C:16]([Cl:20])=[CH:15][N:14]=1)(=[O:11])=[O:10].[CH2:21]([OH:24])[CH:22]=[CH2:23]>>[CH2:21]([O:24][C:18]1[C:13]([NH:12][S:9]([C:3]2[CH:4]=[CH:5][CH:6]=[C:7]([Cl:8])[C:2]=2[Cl:1])(=[O:11])=[O:10])=[N:14][CH:15]=[C:16]([Cl:20])[N:17]=1)[CH:22]=[CH2:23]Participants
3
Procedure
Prepared by the method of Example 31 using allyl alcohol (10 mL) as solvent and 2,3-dichloro-N-(3,5-dichloro-2-pyrazinyl)benzenesulphonamide (Example 74) (0.35 g). Yield 0.32 g.
Sources & evidence
- ORD record
- ord-554618a7683a4ae286de8a7f69638a30
- Source dataset
- uspto-grants-2010_02
- Patent number
- US07662825B2
Reaction notes
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