Cyclopropylamine → HCID 10152373, compound

HRID 1444083Notes

Reaction equation

[Cl:1][C:2]1[C:7]([Cl:8])=[CH:6][CH:5]=[CH:4][C:3]=1[S:9]([NH:12][C:13]1[C:18]([O:19][CH2:20][C:21]2[O:22][C:23]([CH:26]=O)=[CH:24][CH:25]=2)=[N:17][C:16]([Cl:28])=[CH:15][N:14]=1)(=[O:11])=[O:10].[CH:29]1([NH2:32])[CH2:31][CH2:30]1>>[Cl:1][C:2]1[C:7]([Cl:8])=[CH:6][CH:5]=[CH:4][C:3]=1[S:9]([NH:12][C:13]1[C:18]([O:19][CH2:20][C:21]2[O:22][C:23]([CH2:26][NH:32][CH:29]3[CH2:31][CH2:30]3)=[CH:24][CH:25]=2)=[N:17][C:16]([Cl:28])=[CH:15][N:14]=1)(=[O:11])=[O:10]

Participants

Reactant 2

HCID 69828Cyclopropylamine

HCID 10310703HCID 10310703, compound

Product 1

HCID 10152373HCID 10152373, compound

Procedure

Prepared by the method of Example 107b using 2,3-dichloro-N-[5-chloro-3-(5-formyl-2-furanylmethoxy)-2-pyrazinyl]benzenesulphonamide (Example 209) (0.3 g) and cyclopropylamine (0.1 g). Yield 0.1 g.

Workup

customPrepared by the method of Example 107b

Sources & evidence

ORD record: ord-0100f0d2472c49a083c4fa9aba7b30a0
Source dataset: uspto-grants-2010_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07662825B2

Reaction notes

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