HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Phenylfuran-2-carboxylic acid → HCID 59654780, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Phenylfuran-2-carboxylic acid | HCID 736255 | — |
| Reactant | (3-Amino-phenyl)-acetonitrile | HCID 4847850 | — |
| Product | HCID 59654780 | HCID 59654780 | — |
Reaction Steps
5-Phenyl-2-furoic acid (56) (223 mg, 1.2 mmol) was coupled to 3-aminophenyl acetonitrile (80) (157 mg, 1.19 mmol), using Method C. The crude residue was purified by column chromatography, eluting in 17% EtOAc in heptane to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07662839B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-2c4016232832448aa221add33f43f6de |
| Source note | uspto-grants-2010_02 |