HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Aminobenzonitrile → 5-Phenyl-furan-2-carboxylic acid (3-cyano-phenyl)-amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Aminobenzonitrile | HCID 16702 | — |
| Reactant | 5-Phenylfuran-2-carboxylic acid | HCID 736255 | — |
| Product | 5-Phenyl-furan-2-carboxylic acid (3-cyano-phenyl)-amide | HCID 59654679 | — |
Reaction Steps
Carboxylic acid (56) (150 mg, 0.80 mmol) was coupled to 3-amino-benzonitrile (94 mg, 0.80 mmol) using Method C. The residue was purified by column chromatography eluting with 17% EtOAc in heptane to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07662839B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-610c06b622df4d17ad3a399b06acedc3 |
| Source note | uspto-grants-2010_02 |