HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorophenylboronic acid → HCID 59654605, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorophenylboronic acid | HCID 2733986 | — |
| Reactant | HCID 59654866 | HCID 59654866 | — |
| Product | HCID 59654605 | HCID 59654605 | — |
Reaction Steps
The pyridyl bromide (91) (150 mg, 0.47 mmol) was coupled to 3-fluoro-phenylboronic acid (73 mg, 0.52 mmol) using Method E. The crude residue was purified by column chromatography eluting with 20% EtOAc in heptane to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07662839B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-6faf721141984e6f97b625a8403de390 |
| Source note | uspto-grants-2010_02 |