HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorophenylboronic acid → HCID 59654626, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorophenylboronic acid | HCID 2733986 | — |
| Reactant | HCID 59654644 | HCID 59654644 | — |
| Product | HCID 59654626 | HCID 59654626 | — |
Reaction Steps
The pyridyl bromide (77) (100 mg, 0.28 mmol) was coupled to 3-fluoro-phenylboronic acid (42 mg, 0.30 mmol) using Method E. The crude product was purified by column chromatography eluting with 20% EtOAc in heptane to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07662839B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-0c196f2f5b1c43809f0a2b6689e83b8c |
| Source note | uspto-grants-2010_02 |