HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorophenylboronic acid → HCID 59654819, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorophenylboronic acid | HCID 2733986 | — |
| Reactant | HCID 59654854 | HCID 59654854 | — |
| Product | HCID 59654819 | HCID 59654819 | — |
Reaction Steps
The pyridyl bromide (166) (100 mg, 0.26 mmol) was coupled to 3-fluoro-phenylboronic acid (34 mg, 0.24 mmol) using Method E. During this reaction, partial hydrolysis occurred. The residue was extracted using Work-up E1 to give a mixture of acid and ester, which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07662839B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-368512763e454ab795f340b228aad0d9 |
| Source note | uspto-grants-2010_02 |