HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 68679955, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | NoName_3327 | HCID 413085 | — |
| Reactant | HCID 21948865 | HCID 21948865 | — |
| Product | HCID 68679955 | HCID 68679955 | 6% |
Reaction Steps
Analogously to Example 2, the corresponding imine is produced starting from 350 mg of 4-(4-chlorophenyl)-2-hydroxy-4-methyl-2-(trifluoromethyl)pentanal and 158 mg of 4-aminoindazole. By reaction of 50 mg of imine with 1.8 ml of BBr3 (1N in dichloromethane), 29 mg of the title compound is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07662821B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-c4c627eaf8f14602913ff088fb93079c |
| Source note | uspto-grants-2010_02 |