HRID1444658

反应详情

EQUATION

反应方程式

HRID 1444658 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To cefoxitin acid (11 g) in 12% aqueous acetone (88 ml), 60% aqueous sodium lactate (4.7 g) solution was added at 30° C. and stirred for 10 minutes, excess acetone was added (275 ml) to precipitate the product. The solid was filtered and dried under vacuum to yield the title compound in pure form (10 g)

WORKUP

后处理

  1. customto precipitate the product
  2. filtrationThe solid was filtered
  3. customdried under vacuum