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HRID1444680

反应详情

EQUATION

反应方程式

HRID 1444680 的结构方程式

REACTANTS

反应物

1
结构：NC(N)=O.NCCC(=O)O.NCc1ccccc1
HCID86761057

未命名化合物

PRODUCTS

生成物

1
结构：O=C1CCN2C(=O)N(Cc3ccccc3)CCC2N1Cc1ccccc1
HCID46935999

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O=CO
溶剂HCID284

Formic acid

CH2O2

PROCEDURE

实验过程

The thiourea group-containing resin of step (C) was treated with formic acid and kept shaking for 15 hrs. The resin was filtered off and the filtrate was concentrated and purified by chromatography (silica gel) to obtain the title compound.

WORKUP

后处理

  1. filtrationThe resin was filtered off
  2. concentrationthe filtrate was concentrated
  3. custompurified by chromatography (silica gel)