HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → N-(Phenylmethylene)-1-pentanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Pentylamine | HCID 8060 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | N-(Phenylmethylene)-1-pentanamine | HCID 525559 | — |
Reaction Steps
100 g (1.15 mol) N-pentylamine was added to 200 ml methanol at a temperature of 22° C. 121.8 g (1.15 mol) benzaldehyde was added. The mixture was refluxed and subsequently, methanol was distilled off. The residual N-benzylidene-N-pentylamine 199.8 g (99.4%) was used in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07662990B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-6f05789179ec4e2ca629e387abe72d3a |
| Source note | uspto-grants-2010_02 |