HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butanal → 2-Ethylhex-2-Enal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butanal | HCID 261 | — |
| Reactant | 2-Ethylhexanol | HCID 7720 | — |
| Product | 2-Ethylhex-2-Enal | HCID 12582 | — |
Reaction Steps
The production of 2-ethylhexanol (2EH) from normal butyraldehyde (NBD) is being industrially conducted on a large scale. This process is constituted of an NBD condensation step in which two molecules of NBD undergo aldol condensation and dehydration to give 2-ethylhexenal (ethylpropylacrolein, EPA), an EPA hydrogenation step in which the EPA obtained is reacted with hydrogen to obtain crude 2EH, and a 2EH purification step in which the crude 2EH is purified to a desired purity to obtain a 2EH product. The purification of crude 2EH is conducted mainly by distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07663006B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-8d1738cf9372495bbef0fea26db72a01 |
| Source note | uspto-grants-2010_02 |