HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Phenyl-3-Buten-2-one → 4-Phenyl-3-Buten-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Phenyl-3-Buten-2-one | HCID 15909 | — |
| Reactant | Benzyl acetone | HCID 17355 | — |
| Product | 4-Phenyl-3-Buten-2-one | HCID 15909 | — |
| Product | 4-Phenyl-2-butanol | HCID 61302 | — |
Reaction Steps
Next, the reaction product was analyzed by NMR using proton (nuclear magnetic resonance apparatus, hereinafter to be called 1H-NMR). FIG. 5 is a view illustrating the reaction products from hydrogenation reaction of benzalacetone of Example 1. As is obvious from the figure, 4-phenyl-2-butanone and 4-phenyl-2-butanol were obtained by hydrogenation of benzalacetone within five minutes as reaction time at the yield of 97% and 3%, respectively.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07663008B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-61e8d38d8d58494d952e434836a17257 |
| Source note | uspto-grants-2010_02 |