HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-(1,1-Dimethyl-3-methylene-1,3-propanediyl)bisbenzene → Benzene, 1,1'-(1,1,3-trimethyl-1,3-propanediyl)bis-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-(1,1-Dimethyl-3-methylene-1,3-propanediyl)bisbenzene | HCID 80715 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Benzene, 1,1'-(1,1,3-trimethyl-1,3-propanediyl)bis- | HCID 101139 | 100% |
Reaction Steps
In Example 3, hydrogenation reaction was conducted under the same condition as Example 1 for THF diluted solution concentration of the substance to be reduced, its flow rate, and hydrogen 9 flow rate, using 2,4-diphenyl-4-methyl-1-pentene as the substance to be reduced. The reaction time was within five minutes. The analytical result of the reaction product by 1H-NMR showed almost complete hydrogenation of 2,4-diphenyl-4-methyl-1-pentene, and 2,4-diphenyl-2-methylpentane was obtained at about 100% yield (See FIG. 6.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07663008B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-601d242dbd8f4d95b965e9275c47b891 |
| Source note | uspto-grants-2010_02 |