HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Diphenyl-1,3-butadiene → 1,4-Diphenylbutane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Diphenyl-1,3-butadiene | HCID 13452 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 1,4-Diphenylbutane | HCID 66182 | 100% |
Reaction Steps
In Example 4, hydrogenation reaction was conducted under the same condition as Example 1 for THF diluted solution concentration of the substance to be reduced, its flow rate, and hydrogen 9 flow rate, using 1,4-diphenyl-1,3-butadiene as the substance to be reduced. The reaction time was within five minutes. The analytical result of the reaction product by 1H-NMR showed almost complete hydrogenation of 1,4-diphenyl-1,3-butadiene, and 1,4-diphenylbutane was obtained at about 100% yield (See FIG. 6.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07663008B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-257195edaa8348099233e996043efe3f |
| Source note | uspto-grants-2010_02 |