HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1445074Generated: November 2, 2026
1,2,3,4-Tetrahydroisoquinoline → HCID 67141191, compound
https://huagongshe.com/reaction/1445074
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1,2,3,4-Tetrahydroisoquinoline | HCID 7046 | — |
| Reactant | HCID 86615252 | HCID 86615252 | — |
| Product | HCID 67141191 | HCID 67141191 | — |
Reaction Steps
1,2,3,4-Tetrahydroisoquinoline (1 ml) was added to 7-chloro-2-ethyl-3-methyl-1H-pyrrolo[2,3-c]pyridine (850 mg, 4.37 mmol) prepared in Preparation 28. The reaction mixture was stirred overnight at 140° C., cooled to room temperature, and then purified with silica gel column chromatography to give 660 mg of the titled compound as a pale yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07662832B2 |
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| Source dataset | uspto-grants-2010_02 |
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| ORD ID | ord-e3bfeedc05494c52af442ce63ff851c7 |
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| Source note | uspto-grants-2010_02 |
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