HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Nitro-4-toluonitrile → 4-Methyl-2-nitro-thiobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Nitro-4-toluonitrile | HCID 96235 | — |
| Reactant | Thiobenzamide | HCID 683563 | — |
| Reactant | 4-Methyl-2-nitrobenzamide | HCID 13244369 | — |
| Product | 4-Methyl-2-nitro-thiobenzamide | HCID 54168808 | 98% |
Reaction Steps
The thio-benzamide, was prepared as described in Example 14-1, starting from 4-methyl-2-nitro-benzonitrile via 4-methyl-2-nitro-benzamide which gave the title compound (1.03 g, 98%). LC/MS: (Method I): tR=0.54 min, >80%, m/z (ESI)=180 (M-NH2)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07666834B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-9395df17e5504ab898cab1de46807b6f |
| Source note | uspto-grants-2010_02 |