HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 4-(Ethoxycarbonylmethyl)-2-(ethoxycarbonylmethyl)-1,2,4-thiadiazolidine-3,5-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Acetic acid, 2-isothiocyanato-, ethyl ester | HCID 32202 | — |
| Reactant | Ethyl isocyanatoacetate | HCID 76283 | — |
| Reactant | Potassium Permanganate | HCID 516875 | — |
| Product | 4-(Ethoxycarbonylmethyl)-2-(ethoxycarbonylmethyl)-1,2,4-thiadiazolidine-3,5-dione | HCID 11551024 | — |
Reaction Steps
Reagents: Ethyl isothiocyanatoacetate (0.8 ml, 6.5 mmol), 35% HCl (3.1 ml), KMnO4 (0.5 g), ethyl isocyanatoacetate (0.73 ml, 6.5 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07666885B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-af68d21d4695426199c4301500b3556b |
| Source note | uspto-grants-2010_02 |