HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Ethyl 2-(2-methyl-3,5-dioxo-1,2,4-thiadiazolidin-4-yl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | Acetic acid, 2-isothiocyanato-, ethyl ester | HCID 32202 | — |
| Reactant | Potassium Permanganate | HCID 516875 | — |
| Product | Ethyl 2-(2-methyl-3,5-dioxo-1,2,4-thiadiazolidin-4-yl)acetate | HCID 6539175 | — |
Reaction Steps
Reagents: Ethyl isothiocyanatoacetate (0.8 ml, 6.5 mmol), 35% HCl (3.1 ml), KMnO4 (0.5 g), methyl isocyanate (0.38 ml, 6.5 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07666885B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-d355457539e9403bb7f98950292df02b |
| Source note | uspto-grants-2010_02 |