HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid monohydrate → HCID 86614640, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Reactant | (S)-tert-Butyl 3-methoxypyrrolidine-1-carboxylate | HCID 12050278 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86614640 | HCID 86614640 | 141% |
Reaction Steps
Prepare using the method of Intermediate 49 with p-toluenesulfonic acid monohydrate (0.207 g, 1.09 mmol), crude tert-butyl (3S)-3-methoxypyrrolidine-1-carboxylate (See Intermediate 60) (0.50 g, 1.09 mmol) and ethanol (2 mL) to give the title compound as a dark orange coloured oil (0.42 g): MS (m/e): 102 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07666871B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-68881d4685434b7faaf36594ba2f0d88 |
| Source note | uspto-grants-2010_02 |