Triethylamine → HCID 86614641, compound

Participants

Reaction Steps

To a mixture of 2-{5-Methyl-2-[4-(pyridin-2-ylmethoxy)-phenyl]-oxazol-4-yl}-ethanol (0.264 g, 0.85 mmol) and triethylamine (0.154 mL, 1.1 mmol) in CH2Cl2 (4 mL) at 0° C. is added methanesulfonyl chloride (0.077 mL, 1.0 mmol). The mixture is warmed to room temperature and stirred for 2 h. The mixture is concentrated to provide methanesulfonic acid 2-{5-methyl-2-[4-(pyridin-2-ylmethoxy)-phenyl]-oxazol-4-yl}-ethyl ester, which is used without purification. MS (m/e): 389 (M+1)

Provenance & Evidence