HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 68541862, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | N-Methylcyclohexylamine | HCID 7514 | — |
| Reactant | 17beta-Hydroxy wortmannin | HCID 9867340 | — |
| Product | HCID 68541862 | HCID 68541862 | 46% |
Reaction Steps
To a solution of 50 mg (0.12 mmol) 17-hydroxywortmannin in 0.5 mL CH2Cl2 is added 27.2 mg (0.24 mmol) cyclohexyl-methyl-amine. The reaction mixture is stirred at room temperature overnight. CH2Cl2 is removed in vacuo. The residue is triturated with Et2O to give 30 mg (46%) product as an orange powder. MS (ESI) m/z 544.25 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07666901B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-5cec49186997435da892c9b3e1c28462 |
| Source note | uspto-grants-2010_02 |