HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 11699214, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 17beta-Hydroxy wortmannin | HCID 9867340 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 11699214 | HCID 11699214 | 53.3% |
Reaction Steps
To a solution of 50 mg (0.12 mmol) 17-hydroxywortmannin in 0.5 mL CH2Cl2 is added 20.4 mg (0.24 mmol) piperidine. The reaction mixture is stirred at room temperature overnight. CH2Cl2 is removed in vacuo. The residue is triturated with Et2O to give 33 mg (53.3%) product as an orange powder. MS (ESI) m/z 516.25 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07666901B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-c55b1fceb986492998e5856f1f54c32f |
| Source note | uspto-grants-2010_02 |