HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butylamine → HCID 11641892, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butylamine | HCID 6385 | — |
| Reactant | 17beta-Hydroxy wortmannin | HCID 9867340 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 11641892 | HCID 11641892 | 50.1% |
Reaction Steps
To a solution of 100 mg (0.23 mmol) 17-hydroxywortmannin in 2 mL CH2Cl2 is added 49 μL (0.46 mmol) tertbutylamine. The reaction mixture is stirred at room temperature overnight. CH2Cl2 is removed in vacuo. The residue is triturated with Et2O to give 58 mg (50%) product as an orange powder. MS (ESI) m/z 504 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07666901B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-ff3bc86ae12e4f6d93ca50c08573aa77 |
| Source note | uspto-grants-2010_02 |