HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethyl-1,3-propanediamine → HCID 11541064, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethyl-1,3-propanediamine | HCID 7993 | — |
| Reactant | 17beta-Hydroxy wortmannin | HCID 9867340 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 11541064 | HCID 11541064 | 60.4% |
Reaction Steps
To a solution of 100 mg (0.23 mmol) 17-hydroxywortmannin in 2 mL CH2Cl2 is added 58 μL (0.46 mmol) N,N-dimethyl-1,3-propanediamine. The reaction mixture is stirred at room temperature overnight. CH2Cl2 is removed in vacuo. The residue is triturated with Et2O to give 74 mg (60%) product as an orange powder. MS (ESI) m/z 533 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07666901B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-6c257cb0ec3a4530bf5b740c4c585308 |
| Source note | uspto-grants-2010_02 |