HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 44242401, compound → HCID 44242402, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 44242401 | HCID 44242401 | — |
| Solvent | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Product | HCID 44242402 | HCID 44242402 | 88.3% |
Reaction Steps
To a solution of (S,S)—N-(3-{3-Fluoro-4-[4-(4-methoxy-benzyloxy)-2-(2-nitro-6,7-dihydro-5H-imidazo[2,1-b][1,3]oxazin-6-yloxy)-pyrimidin-5-yl]-phenyl}-2-oxo-oxazolidin-5-ylmethyl)-acetamide (60 mg, 0.092 mmol) in TFA/methylene chloride (3.0 mL, 1/1) was stirred at rt for 1 h. Solvents were evaporated and triturated with ether to give the title product (43 mg, 88%) as a pale yellow solid. ESI MS m/z 530.4 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07666864B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-06348da3bd2244fe949b383c3bb7a780 |
| Source note | uspto-grants-2010_02 |