HRID1446251

反应详情

EQUATION

反应方程式

HRID 1446251 的结构方程式

PROCEDURE

实验过程

The title compound was prepared from 5-(4-trifluoromethylphenyl)isoxazole-4-carboxylic acid (12.9 mg, 0.050 mmol) and 3-[4-(trifluoromethyl)phenyl]pyrrolidine oxalate (18.3 mg, 0.060 mmol) as described in synthetic method C and thereafter purified by preparative HPLC method B to give a solid (5.5 mg). Calcd for C22H16F6N2O2: 454.1116, found 454.1116.

WORKUP

后处理

  1. custompurified by preparative HPLC method B