3-(Pyrrolidin-3-yl)pyridine → HCID 23658555, compound

Participants

Reaction Steps

To 5-(4-methylphenyl)isoxazole-4-carbonyl chloride (15 mg, 0.068 mmol) in dichloromethane (1 mL) was added 3-pyrrolidin-3-ylpyridine (11 mg, 0.074 mmol, 1.1 eq.), and the reaction mixture was stirred for 1 h. The solvent was removed, and the residue was purified by preparative reverse-phase HPLC to give the title compound. HRMS (ESI, pos. ion) m/z calcd for C20H19N3O2: 333.1477, found 333.1471.

Provenance & Evidence