HCID 11528691, compound → HCID 13021077, compound

HRID 1446808Notes

Reaction equation

HRID 1446808 reaction equation
[NH2:1][N:2]1[CH2:8][CH2:7][CH2:6][C:5]2[CH:9]=[CH:10][CH:11]=[CH:12][C:4]=2[C:3]1=O.C(O[C:17](=[NH:30])[C:18]1[CH:23]=[CH:22][C:21]([C:24]2[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=2)=[CH:20][CH:19]=1)C>C(OCC)C>[C:21]1([C:24]2[CH:25]=[CH:26][CH:27]=[CH:28][CH:29]=2)[CH:20]=[CH:19][C:18]([C:17]2[N:30]=[C:3]3[C:4]4[CH:12]=[CH:11][CH:10]=[CH:9][C:5]=4[CH2:6][CH2:7][CH2:8][N:2]3[N:1]=2)=[CH:23][CH:22]=1

Participants

4

Reactant 2

HCID 11528691HCID 11528691, compoundHCID 13021078HCID 13021078, compound

Product 1

HCID 13021077HCID 13021077, compoundYield 63%

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

This compound was prepared according to the procedure of Example 3 starting from 2-amino-4,5-dihydro-2-benzazepine-1(2H,3H)-one and 4-phenyl-benzimidic acid ethyl ester. Yield 63%. M.p. 135°-37° C. (from diethyl ether).

Workup

  1. customThis compound was prepared

Sources & evidence

ORD record
ord-6f4dd820081d45fd8d0f0244a912837e
Source dataset
uspto-grants-1982_02
Patent number
US04313950

Reaction notes

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