Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylamine → 2-(2-(2-(Dimethylamino)ethoxy)ethoxy)ethanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylamine | HCID 674 | — |
| 반응물 | 2-(2-(2-Chloroethoxy)ethoxy)ethanol | HCID 78871 | — |
| 생성물 | 2-(2-(2-(Dimethylamino)ethoxy)ethoxy)ethanol | HCID 10845034 | — |
반응 단계
Commercial Cl(CH2CH2O)3H (abb. ClE3H) (2.0 mole) and dimethylamine (20.0 mole) were mixed in a flask (3.0 l) fitted with a condenser and stirred (RT) for 30 hours. TLC (Si-gel) examination showed the complete consumption of the ClE3H. Excess dimethylamine was removed by two consecutive evaporations under reduced pressure. The residual material was reconstituted in CHCl3, dried (MgSO4), filtered and evaporated to dryness to produce the product, 8-dimethylamino-3,6-dioxaoctanol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04314060 |
| 출처 데이터셋 | uspto-grants-1982_02 |
| ORD ID | ord-431be094b9644bce8e2107c02042c0cd |
| 출처 메모 | uspto-grants-1982_02 |