HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic acid 10-acetoxymethyl-anthracen-9-ylmethyl ester → HCID 12803438, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic acid 10-acetoxymethyl-anthracen-9-ylmethyl ester | HCID 613145 | — |
| Reactant | HCID 12803422 | HCID 12803422 | — |
| Product | HCID 12803438 | HCID 12803438 | — |
Reaction Steps
Approximately 21.8 g of 1-(2-methoxyethyl)-4-phenyl-4-imidazolin-2-one and 120 ml. of acetic anhyride is refluxed together for four hours. The acetic anhydride is distilled out at reduced pressure. The residual semisolid is recrystallized from ether to yield the title compound as a white solid; m.p. 73°-75° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04314066 |
| Source dataset | uspto-grants-1982_02 |
| ORD ID | ord-e8362b7ec9ca4753b627fdb170193b6a |
| Source note | uspto-grants-1982_02 |