HuagongsheHuagongshe Chemistry Print Report · For research reference only
n-Methyl-p-aminophenol → HCID 13314817, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | n-Methyl-p-aminophenol | HCID 5931 | — |
| Reactant | 4-[N-methyl-N-(5-chloro-2-benzothiazolyl)amino]phenol 2,5-Dichlorobenzothiazole | HCID 20553509 | — |
| Solvent | Acetonitrile--water (1/1) | HCID 18373917 | — |
| Product | HCID 13314817 | HCID 13314817 | 170.2% |
Reaction Steps
4-[N-methyl-N-(5-chloro-2-benzothiazolyl)amino]phenol 2,5-Dichlorobenzothiazole (5.0 g) and 4-(N-methylamino)phenol (4.7 g) were added to a water/acetonitrile mixture (1:1) and the mixture was heated under reflux for a period of 24 hours. After cooling the solid was collected by filtration and recrystallised from water/acetonitrile to give 4-[N-methyl-N-(5-chloro-2-benzothiazolyl)amino]phenol (5.0 g) as colourless crystals, mp 238°-240° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04314065 |
| Source dataset | uspto-grants-1982_02 |
| ORD ID | ord-3173f3d3bd654d0a90bb8d4f33798502 |
| Source note | uspto-grants-1982_02 |