Ethanolamine → HCID 20553427, compound
Reaction equation
Cl.Cl[CH2:3][CH2:4][O:5][C:6]1[CH:7]=[CH:8][C:9]2[C:18]([CH:19]=1)=[N:17][C:16]1[C:11](=[CH:12][CH:13]=[C:14]([O:20][CH2:21][CH2:22]Cl)[CH:15]=1)[CH:10]=2.[CH2:24]([CH2:26][NH2:27])[OH:25]>>[OH:25][CH2:24][CH2:26][NH:27][CH2:3][CH2:4][O:5][C:6]1[CH:7]=[CH:8][C:9]2[C:18]([CH:19]=1)=[N:17][C:16]1[C:11](=[CH:12][CH:13]=[C:14]([O:20][CH2:21][CH2:22][NH:27][CH2:26][CH2:24][OH:25])[CH:15]=1)[CH:10]=2Participants
3
Procedure
The compound is prepared from 3,6-bis(2-chloroethoxy)acridine hydrochloride and ethanolamine as described in Example 15, giving 0.7 g. of the desired product as yellow crystals, m.p. 125°-127° C.
Workup
- customgiving 0.7 g
Sources & evidence
- ORD record
- ord-443bd2e1e49c4009be68f1e04c3bc55c
- Source dataset
- uspto-grants-1982_02
- Patent number
- US04314061
Reaction notes
Loading…