HCID 20553441, compound → HCID 20553426, compound

HRID 1446909Notes

Reaction equation

HRID 1446909 reaction equation
[NH2:1][CH2:2][CH2:3][O:4][C:5]1[CH:6]=[CH:7][C:8]2[C:17]([CH:18]=1)=[N:16][C:15]1[C:10](=[CH:11][CH:12]=[C:13]([O:19][CH2:20][CH2:21][NH2:22])[CH:14]=1)[CH:9]=2.[C:23](OC(=O)C)(=[O:25])[CH3:24].[C:30](O)(=[O:32])[CH3:31]>>[C:23]([NH:22][CH2:21][CH2:20][O:19][C:13]1[CH:12]=[CH:11][C:10]2[C:15]([CH:14]=1)=[N:16][C:17]1[C:8](=[CH:7][CH:6]=[C:5]([O:4][CH2:3][CH2:2][NH:1][C:30](=[O:32])[CH3:31])[CH:18]=1)[CH:9]=2)(=[O:25])[CH3:24]

Participants

3

Reactant 2

HCID 20553441HCID 20553441, compoundHCID 21895370AcOH AcOAc

Product 1

HCID 20553426HCID 20553426, compound

Procedure

3,6-bis(2-aminoethoxy)acridine is treated with acetic anhydride/acetic acid followed by in vacuo removal of the volatiles, giving, after crystallization, the desired product.

Workup

  1. customfollowed by in vacuo removal of the volatiles
  2. customgiving
  3. customafter crystallization

Sources & evidence

ORD record
ord-663a23598ba44bfb994f0b57da223ec3
Source dataset
uspto-grants-1982_02
Patent number
US04314061

Reaction notes

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