3,6-Bis(2-(diethylamino)ethoxy)acridine → HCID 86738236, compound

HRID 1446914Notes

Reaction equation

HRID 1446914 reaction equation
[CH2:1]([N:3]([CH2:29][CH3:30])[CH2:4][CH2:5][O:6][C:7]1[CH:8]=[CH:9][C:10]2[C:19]([CH:20]=1)=[N:18][C:17]1[C:12](=[CH:13][CH:14]=[C:15]([O:21][CH2:22][CH2:23][N:24]([CH2:27][CH3:28])[CH2:25][CH3:26])[CH:16]=1)[CH:11]=2)[CH3:2].[Cl-:31].[Zn+2:32].[Cl-]>C(O)C>[Cl-:31].[Zn+2:32].[CH2:27]([N:24]([CH2:25][CH3:26])[CH2:23][CH2:22][O:21][C:15]1[CH:14]=[CH:13][C:12]2[C:17]([CH:16]=1)=[N:18][C:19]1[C:10](=[CH:9][CH:8]=[C:7]([O:6][CH2:5][CH2:4][N:3]([CH2:29][CH3:30])[CH2:1][CH3:2])[CH:20]=1)[CH:11]=2)[CH3:28].[Cl-:31]

Participants

4

Reactant 2

HCID 1625413,6-Bis(2-(diethylamino)ethoxy)acridineHCID 3007855Zincchloride

Product 1

HCID 86738236HCID 86738236, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A suspension of 3,6-bis(2-diethylaminoethoxy)acridine free base and one equivalent of zinc chloride in ethanol is refluxed for 2 hours. The mixture is precipitated with ethyl acetate giving the 1:1 complex.

Workup

  1. temperatureis refluxed for 2 hours
  2. customThe mixture is precipitated with ethyl acetate giving the 1:1 complex

Sources & evidence

ORD record
ord-a28556f2f6684481a26482e6d92e8d77
Source dataset
uspto-grants-1982_02
Patent number
US04314061

Reaction notes

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