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Toluene → 2-Ethylhexanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Toluene | HCID 1140 | — |
| 反応物 | Diisocyanatotoluene | HCID 12905475 | — |
| 生成物 | 2-Ethylhexanol | HCID 7720 | — |
反応手順
The batch is then diluted with 185.0 parts of toluene and a mixture of 180.0 parts of the semi-blocked toluylene diisocyanate referred to in Example 1 and 150.0 parts of a semi-blocked toluylene diisocyanate obtained from 2-ethylhexanol and an 80/20 toluylene diisocyanate isomer mixture is added in the course of 2 hours 15 minutes at 90° C. After completion of this addition, stirring is continued for 1 hour at 90° C., and the mixture is then heated to 120° C., kept at this temperature for 3.5 hours, and diluted after cooling with 81 parts of toluene. The solids content of the resulting polyether-polyol derivative containing blocked isocyanate groups, ie. of component A, is 71%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04315840 |
| 出典データセット | uspto-grants-1982_02 |
| ORD ID | ord-f4c01a232af541f68c1497a6022e0e4d |
| 出典メモ | uspto-grants-1982_02 |