Sodium Hydroxide → HCID 13156310, compound

HRID 1447166Notes

Reaction equation

HRID 1447166 reaction equation
C([N:5]1[C:10]2=[N:11][N:12]=[CH:13][N:9]2[C:8]2[CH:14]=[CH:15][CH:16]=[CH:17][C:7]=2[N:6]1[C:18](=[O:21])[CH2:19][CH3:20])(=O)CC.[OH-].[Na+]>>[C:18]([N:6]1[C:7]2[CH:17]=[CH:16][CH:15]=[CH:14][C:8]=2[N:9]2[CH:13]=[N:12][N:11]=[C:10]2[NH:5]1)(=[O:21])[CH2:19][CH3:20]

Participants

3

Reactant 2

HCID 14798Sodium HydroxideHCID 13156309HCID 13156309, compound

Product 1

HCID 13156310HCID 13156310, compoundYield 64.2%

Procedure

5.0 g (0.017 mole) of 4,5-dipropionyl-4,5-dihydro-s-triazolo[3,4-c]benzo-as-triazine are treated with 50 ml of a 5% sodium hydroxide solution. The solution which forms within a short time is decolourized, filtered, the filtrate is acidified with acetic acid, and the separated colourless precipitate is filtered off. 2.5 g (63%) of the title compound are obtained; m.p.: 244° C.

Workup

  1. filtrationfiltered
  2. filtrationthe separated colourless precipitate is filtered off

Sources & evidence

ORD record
ord-31ed1cd7a63045719532758f3982684f
Source dataset
uspto-grants-1982_02
Patent number
US04316022

Reaction notes

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